微细粒低品位钽铌锂资源综合回收新工艺实验

    Experiment on New Comprehensive Recovery of Micro-fine Particle Low-grade Refractory Tantalum Niobium Lithium Resources

    • 摘要: 宜春钽铌矿微细粒低品位尾泥含Li2O为0.17%,含Ta2O5为0.007 1%,含Nb2O5为0.007 8%,白度为24.20%,工艺矿物学研究显示,该尾泥中钽铌矿物与锂云母粒度小于-20 μm,长石粒度小于-45 μm,属微细粒低品位矿物,资源回收较为困难。通过采用“浆料机磁选除铁—悬振锥面回收钽铌—浮选提高长石白度—浮选回收锂云母”选矿工艺流程对该尾泥进行综合回收,实验获得钽铌精矿(TaNb)2O5品位为27.75%,锂云母精矿Li2O品位1.57%,回收率42.76%;长石Al2O3品位14.92%,Fe2O3品位为0.045%,白度为68.70%,钾钠合量为7.91%,实现了钽铌、锂、长石资源的综合回收。

       

      Abstract: The fine-grained low-grade tail mud of the Yichun tantalum niobium ore contains 0.17% Li2O, 0.007 1% Ta2O5, 0.007 8% Nb2O5, and whiteness is 24.20%. Mineralogical studies indicate that tantalum-niobium minerals and lithium mica particles in the tailings are mainly distributed below -20 μm, while feldspar particles are mainly distributed below -45 μm, which is a fine grained and low grade mineral, making resource recovery challenging. Through the beneficiation process of "slurry magnetic separation for iron removal-vibrating cone recovery of tantalum-niobium-flotation to improve feldspar brightness-flotation recovery of lithium mica for the comprehensive recovery of this tailings, experiments achieved a tantalum-niobium concentrate (TaNb)2O5 grade of 27.75%, lithium mica concentrate Li2O grade of 1.57%, with a recovery rate of 42.76%. The feldspar had an Al2O3 grade of 14.92%, Fe2O3 grade of 0.045%, brightness of 68.70%, and total alkali content of 7.91%. This process successfully achieved comprehensive recovery of tantalum-niobium, lithium, and feldspar resources.

       

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